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Last 4!

4d - be angry, having to swallow a certain pungent liquid (4, 3) B*N* O*L

46d - wretched fold are truning up fully clother? (7) T*E***S

52d - in ancient language play on words isn't comprehensible at first (5) P***C POWIC?

54a - most unusual being suppplied with both question and answer in exam (9)
QU****E*T

Thanks in advance

54ac Quaintest maybe.

Thanks

52d is PUNIC
46d is TOERAGS
Still unsure about 4d

Could it be bone oil - boil + one?

4d bone oil

quaintest
bone oil
toerags
punic